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      STA同步热分析仪软件使用方法
      2017-09-20 17:10:02
      1. 打开软件界面如下:选择文件—新建。

      打开新建出现下图;按照参数一一填写,其中坩埚质量填写步骤:仪器开机5分钟左右,将空坩埚放入炉体中间,仪器界面TG数据开始增加。稳定三个小?#20445;?#24453;仪器显示屏上TG质量稳定正负0.10?#37327;耍?#23558;数据填写框中。然后取出坩埚,放入样品,再次放入炉体中,待TG数据稳定正负0.10?#37327;耍?#23558;数据填写在称重质量表格中,这时样?#20998;?#37327;自动显示出来。测量类型选择样品加修正,仪器类型选择STA,其他根据情况填写。然后连接仪器,仪器会有滴?#21335;?#22768;,通讯连接成功,然后点继续。注(样品一栏必须填写否则无法实验)

      2.继续以后出现下图所示,终止温度(室温-1000度之间,根据样品选择合适温度)

      3.扫描速率一般10|min℃和20|min℃。选择设置,退出。

      4.开始实验。选择测量-开始测量即可。如下图所示。

      5.到达设置温度,仪器自动停止,绿色为TG质量线,蓝色为DSC曲线。横坐标为温度、左侧纵坐标为质量坐标、右侧纵坐标为DSC坐标(坐标大小在设置里选择可调坐标抽选择合适的区间)实验结束,选择保存—存为样品即可,如下图所示。

      6.选择数据分析—质量变化—如图所示.注(根据需要选择相应的分析结果)

      7.页面出现变化如图所示

      8.调节左右两根黑线,选择温度范围,确定范围后选择应用,出现下图所示;失重质量百分比得出。实验结束。


      9.生成报告-打印。选择文件—打印预览即可。如下图所示;


         
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